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- W2012735897 abstract "Abstract The synthesis and characterisation of some anionic Ni, Pd and Pt complexes of the ligand, Na2C3S5, (C3S52− = 1,3-dithiole-2-thione-4,5-dimercapto = dmit) are reported. The complexes were isolated as PPN+ [PPN+ = bis(triphenylphosphine)iminium] salts. The monoanionic complexes [PPN] [Ni(C3S5)2] and [PPN] [Pd(C3S5)2] were further oxidised with iodine in acetonitrile to afford [PPN]0.25[Ni(C3S5)2] and [PPN]0.25 [Pd(C3S5)2]. The partially oxidised complexes have electrical conductivities of 1.2 × 10−2 and 0.64 S cm−1 at room temperature for compacted pellets. Cyclic voltammetry, electronic, IR and ESR spectra of the complexes are discussed. A single crystal X-ray determination of [PPN] [Ni(C3S5)2]·MeOH was carried out. The average value of NiS bond length is one of the highest observed for a [Ni(dmit)2] complex" @default.
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- W2012735897 title "Synthesis and characterisation of some [M(C3S5)2]n− complexes (M = Ni, Pd, Pt). Single crystal structure of [PPN] [Ni(C3S5)2] · MeOH" @default.
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