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- W2012743485 abstract "Two copper–molybdenum bronzes: CuyMoO3−z (0.1 < y < 0.2; typically y ∼ 0.15) and CuxMoO3 (0.2 < x < 0.25; typically x ∼ 0.23) were prepared as glistening black polycrystalline materials by the solid state reaction of Cu and MoO3 at 600 °C under argon in Pt crucibles. Powder XRD showed that the material with global composition ‘0.1Cu·MoO3’ comprises ∼Cu0.15MoO3 and MoO3; whilst ‘0.2Cu·MoO3’ comprises ∼Cu0.15MoO3 and ∼Cu0.23MoO3. DTA performed on ‘0.2Cu·MoO3’ reveals a reversible solid state phase transition ∼520 °C under argon. Reacting equimolar amounts of Cu2O and MoO2 at 600 °C in a Cu crucible under argon yields: Cu6Mo5O18, Cu and MoO2. A tentative subsolidus Cu–MoO2–O isothermal (∼25 °C) phase diagram under argon is drawn from these data. Oxidation states of Cu and Mo within this system are discussed." @default.
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- W2012743485 date "2010-11-01" @default.
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- W2012743485 title "On the coexistence of copper–molybdenum bronzes: CuxMoO3 (0.2<x<0.25; typically x∼0.23) and CuyMoO3−z (0.1<y<0.2; typically y∼0.15) in the Cu–MoO2–O quasi-ternary system" @default.
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- W2012743485 doi "https://doi.org/10.1016/j.materresbull.2010.07.004" @default.
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