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• W2012775856 startingPage "3213" @default.
• W2012775856 abstract "Lignocellulosic biomass is composed of the polysaccharides cellulose and hemicellulose and the polyphenol lignin. Many current methods for analyzing the structure of lignocelluloses involve a sequential extraction of the material and subsequent analysis of the resulting fractions, which is labor-intensive and time-consuming. The work presented here assesses the dissolution of whole lignocellulosic material, focusing on biomass derived from the perennial bioenergy grass Miscanthus. The solvent dimethylsulfoxide (DMSO)-d6 containing 1-ethyl-3-methylimidazolium acetate ([Emim]OAc) was able to dissolve lignocellulosic material completely and gave high-resolution 2D heteronuclear single quantum coherence (HSQC) NMR spectra of the entire array of wall polymers. Extrapolated time-zero HSQC was applied using DMSO-d6/[Emim]OAc-d14 and enabled quantitative analysis of structural traits of lignocellulose components." @default.
• W2012775856 created "2016-06-24" @default.
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• W2012775856 date "2013-03-04" @default.
• W2012775856 modified "2023-09-25" @default.
• W2012775856 title "Solution-State 2D NMR Spectroscopy of Plant Cell Walls Enabled by a Dimethylsulfoxide-<i>d</i>₆/1-Ethyl-3-methylimidazolium Acetate Solvent" @default.
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• W2012775856 doi "https://doi.org/10.1021/ac303529v" @default.
• W2012775856 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23413964" @default.
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