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- W2012805321 abstract "Abstract The comparative kinetic analysis of the non-isothermal crystallization was performed for Eu 3 + doped Zn 2 SiO 4 samples, prepared by the polymer induced sol–gel procedure and thermally treated in the conventional furnace and in a microwave oven. This comparison is done using various thermal analysis techniques and is supported by SEM investigation. It was found that low values of Avrami constant ( n ), identified in the primary crystallization stage resulted from a not constant radial growth rate. One possible mechanism that could alter the linear crystal growth rate is a diffusion-controlled transition, with instantaneous nucleation mechanism. In the secondary crystallization stage, observed for both samples, it was found that the probability for two-dimensional crystal growth increases, especially at higher heating rates. It was found that the substitution of zinc ions by europium ions in Zn 2 SiO 4 matrix can lead to some defects due to different radius and charges, which induces autocatalytic behavior of the tested systems. It was shown that the two-parameter Sestak–Berggren (SB) autocatalytic model best describes the non-isothermal crystallization of doped samples. It has been shown that SB model is adequate to describe the crystallization kinetics for the fine powder samples (crystallite size of 60–65 nm)." @default.
- W2012805321 created "2016-06-24" @default.
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- W2012805321 date "2013-11-01" @default.
- W2012805321 modified "2023-10-15" @default.
- W2012805321 title "The comparative kinetic analysis of the non-isothermal crystallization process of Eu3+ doped Zn2SiO4 powders prepared via polymer induced sol–gel method" @default.
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- W2012805321 doi "https://doi.org/10.1016/j.powtec.2013.09.020" @default.
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