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• W2012809462 abstract "The formation of inclusion complexes between the native cyclodextrins (CDs) and the urea herbicide cycluron has been investigated both in solution and in the solid state. Single-crystal X-ray structures of both the uncomplexed guest and the β-CD·cycluron complex were determined while powder X-ray diffraction was used to confirm complexation between γ-CD and cycluron in the solid state. Solution-state complexation between the herbicide and α-, β- and γ-CD was established using 1H NMR spectroscopy and isothermal titration calorimetry (ITC). From the 1H NMR spectroscopic studies 1:1 complex stoichiometry was indicated in all cases and association constant values (K) were determined as 228, 3254 and 155 for the complexes α-CD·cycluron, β-CD·cycluron and γ-CD·cycluron, respectively. Assigning a 1:1 host–guest ratio, the ITC technique produced K values of the same order as those determined using the spectroscopic method. The thermodynamic parameters ΔH, ΔS and ΔG obtained using ITC provide insights into the dri..." @default.
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• W2012809462 date "2012-04-27" @default.
• W2012809462 modified "2023-09-26" @default.
• W2012809462 title "Investigation of the inclusion of the herbicide cycluron in native cyclodextrins by X-ray diffraction, nuclear magnetic resonance spectroscopy and isothermal titration calorimetry" @default.
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• W2012809462 doi "https://doi.org/10.1080/10610278.2012.676180" @default.
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