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- W2012842000 abstract "Two novel polyphosphides, NaP5 and CeP5, were prepared in a BN crucible by the reaction of elemental components under a high pressure of 3 GPa at 800–950 °C. The X-ray structural analysis showed that NaP5 crystallizes in an orthorhombic space group Pnma with a=10.993(2) Å, b=6.524(1) Å, c=6.903(1) Å, Z=4 and CeP5 in the monoclinic group P21/m with a=4.9143(5) Å, b=9.6226(8) Å, c=5.5152(4) Å, β=104.303(6)°, Z=2. The crystal structure of NaP5 consists of a three-dimensional framework ∞3[P5]1− constructed by PP bonds among four crystallographically inequivalent phosphorus sites, with large channels hosting the sodium cations, while CeP5 is a layered compound containing ∞2[P5]3− polyanionic layers that are separated by Ce3+ ions. NaP5 exhibits the diamagnetic behavior, while the temperature-dependent magnetic susceptibility of CeP5 essentially follows the Curie–Weiss law." @default.
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- W2012842000 date "2004-05-01" @default.
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- W2012842000 title "High-pressure synthesis and crystal structures of two new polyphosphides, NaP5 and CeP5" @default.
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- W2012842000 doi "https://doi.org/10.1016/j.jallcom.2003.09.107" @default.
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