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- W2012853917 abstract "2-Bromopyridine reacts with elemental phosphorus (red or white) in a superbasic KOH/DMSO(H2O) suspension at 100 °C (for red phosphorus) and 75 °C (for white phosphorus) over 3 h to afford tris(2-pyridyl)phosphine in a 62% yield (from red phosphorus) and a 50% yield (from white phosphorus). Under microwave assistance, the reaction with red phosphorus takes just 20 min to produce tris(2-pyridyl)phosphine in 53% yield. A hitherto unknown complex, [Pd(PPy3)2Cl2]·CH2Cl2, synthesized from tris(2-pyridyl)phosphine and PdCl2, has the cis-configuration; this is unusual for bis(phosphino)palladium dichloride complexes." @default.
- W2012853917 created "2016-06-24" @default.
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- W2012853917 date "2012-05-01" @default.
- W2012853917 modified "2023-09-23" @default.
- W2012853917 title "Expedient one-pot organometallics-free synthesis of tris(2-pyridyl)phosphine from 2-bromopyridine and elemental phosphorus" @default.
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- W2012853917 doi "https://doi.org/10.1016/j.tetlet.2012.03.004" @default.
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