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• W2012874872 abstract "Abstract Models describing the retention of small molecules combined with the additivity rules for the contributions to the retention can be used for prediction of the retention and resolution of oligomers, small synthetic polymers and copolymers in interactive liquid chromatography with dependency on the molar mass distribution and on the composition of the mobile phase, both in reversed-phase and in normal-phase chromatographic systems, for isocratic or gradient elution. Synthetic copolymers or cooligomers with two (or more) repeat monomer units show not only molar mass distribution, but also composition and sequence distribution of the individual repeat units. By combination of adequately selected separation conditions in normal-phase and in reversed-phase systems, the separation conditions can be adjusted to enhance or to suppress the chromatographic resolution according to each of the two distribution modes and to achieve the separation following the distribution of any of the two repeating groups under “critical conditions” of interactive HPLC. The sequence distribution, i.e., the distribution of the position of the blocks was found to affect significantly the retention behavior of the individual species in the block cooligomers. Based on the retention mechanism suggested, optimization of the conditions for isocratic and gradient-elution separations of cooligomers is possible. Key Words: CopolymersCooligomersInteractive liquid chromatographyOligoethylene glycol derivatives" @default.
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• W2012874872 date "2001-02-01" @default.
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• W2012874872 title "Retention Behavior of Oligomers and Cooligomers in Reversed-phase and in Normal-phase Interactive Liquid Chromatographic Systems" @default.
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• W2012874872 doi "https://doi.org/10.1080/10236660108033948" @default.
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