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- W2013081572 abstract "Under suitable conditions, PCL5 reacts and quantitatively with NH4Cl to form [Cl3P = N–PCl3] [PCl6], which, with additional PCl5 and NH4Cl, is transformed to [Cl3P = N–PCl2 = N–PCl3] [PCl6].The cation of the latter compound and the NH ion react with ring closure to form [NPCl2]3, together with longer chains which can yield with NH either [NPCl2]4 or, for example, Cl3P = N-(PCl2 = N) n-PCl2 = NH. The salt-like intermediates of the phosphonitrilic chloride synthesis react with S02 to form the oxygen-containing products, Cl3P = N–P(O)Cl2 and Cl3P = N–PCl2 = N–P(O)Cl2. Sulfur analogs are also easily obtained. The constitution of the compounds was determined by nuclear magnetic reasonance spectroscopy." @default.
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- W2013081572 date "1962-06-01" @default.
- W2013081572 modified "2023-10-16" @default.
- W2013081572 title "Phosphonitrilic Chlorides from Phosphorus Pentachloride" @default.
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- W2013081572 doi "https://doi.org/10.1002/anie.196202811" @default.
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