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• W2013094844 abstract "Semiconducting icosahedral boron arsenide, B 12 As 2 , is an excellent candidate for neutron detectors, thermoelectric converters, and radioisotope batteries, for which high quality single crystals are required. Thus, the present study was undertaken to grow B 12 As 2 crystals by precipitation from metal solutions (nickel) saturated with elemental boron (or B 12 As 2 powder) and arsenic in a sealed quartz ampoule. B 12 As 2 crystals of 10-15 mm were produced when a homogeneous mixture of the three elements was held at 1150 °C for 48-72 h and slowly cooled (3.5 °C/h). The crystals varied in color and transparency from black and opaque to clear and transparent. X-ray topography (XRT), and elemental analysis by energy dispersive X-ray spectroscopy (EDS) confirmed that the crystals had the expected rhombohedral structure and chemical stoichiometry. The concentrations of residual impurities (nickel, carbon, etc.) were low, as measured by Raman spectroscopy and secondary ion mass spectrometry (SIMS). Additionally, low etch-pit densities (4.4 x 10 7 cm ―2 ) were observed after etching in molten KOH at 500 °C. Thus, the flux growth method is viable for growing large, high-quality B 12 As 2 crystals." @default.
• W2013094844 created "2016-06-24" @default.
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• W2013094844 date "2011-03-01" @default.
• W2013094844 modified "2023-09-26" @default.
• W2013094844 title "Semiconducting icosahedral boron arsenide crystal growth for neutron detection" @default.
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• W2013094844 doi "https://doi.org/10.1016/j.jcrysgro.2010.10.057" @default.
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