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• W2013291392 abstract "Abstract The preparation of 4′-alkyl- and 4′-alkoxy-4-cyano-3-fluorobiphenyls by four different procedures is described and discussed; the best method involves palladium(0)-catalysed coupling of arylboronic acids and 4-bromo-(or 4-iodo-)-2-fluorobenzonitrile. The effects on transition temperatures of fluoro substitution ortho to the terminal cyano group in biphenyls are compared with the effects in other terminal cyano compounds and in mesogens without a terminal cyano group. The effect of the ortho fluoro substituent in 4-cyanobiphenyls is particularly large and is probably due to the severe disruption of antiparallel correlations; the depressions of the smectic A and nematic phase stabilities are similar which suggests that, as for compounds with alkyl or alkoxy terminal groups, the fluoro substituent at the 3-position has a tendency to enhance smectic character, but this is offset by the molecular broadening it causes." @default.
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• W2013291392 date "1995-07-01" @default.
• W2013291392 modified "2023-10-01" @default.
• W2013291392 title "The synthesis and transition temperatures of some 4′-alkyl- and 4′-alkoxy-4-cyano-3-fluorobiphenyls" @default.
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• W2013291392 doi "https://doi.org/10.1080/02678299508036722" @default.
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