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- W2013345697 abstract "The synthesis of 5-methoxyuridine (3), 5-methoxycytidine (6), 1-(2-deoxy-β-D-erythropento-furanosyl)-5-methoxyuracil (14), 5-methoxy-1-β-D-ribofuranosyl-4-thiopyrimidin-2-one (5), 1-β-D-arabinofuranosyl-5-methoxycytosine (12), 1-β-D-arabinofuranosyl-5-methoxyuracil (8) and 1-β-D-arabinofuranosyl-5-methoxy-4-thiopyrimidin-2-one (11) have been accomplished. Both 3 and 14 were synthesized by alkylation of 2,4-bis(trimethyIsilyI)-5-methoxyuracil (1) with the appropriately blocked halosugars. Synthesis of the corresponding 5-methoxy-1-β-D-arabinofuranosyl derivatives was accomplished through the intermediate 2,2 -anhydro-1-β-D-arabinofuranosyl-5-methoxyuracil (7). The cytosine and 4-thiouracil derivatives in both the arabino- and ribo- series were prepared by thiation followed by amination." @default.
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- W2013345697 title "The synthesis of some 5-methoxypyrimidine nucleosides" @default.
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