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- W2013372014 abstract "Polyfluoroazoxyarenes [RC6F4·N(O):N·C6F4R; R = F, p-H, or o-H] are obtained in high yield (>90%) by oxidation of the corresponding azo-compounds with trifluoroperacetic acid. Decafluoroazoxybenzene is substituted at the 2- or 4-position in the ring adjacent to the [graphic omitted]–[graphic omitted] group when treated with aqueous ethanolic ammonia, and the azoxy-compounds undergo reductive cleavage to amines and/or diamines on treatment with hydriodic acid. The reactions of azoxypolyfluoroarenes with hydrazine hydrate yield 1-anilinobenzotriazoles. Tetrafluorobenzotriazole itself may be obtained by reduction of the 1-pentafluoroanilino-compound or of tetrafluorobenzotriazol-1-ol with hydriodic acid, or by treatment of tetrafluoro-o-phenylenediamine with nitrous acid. Tetrafluorobenzotriazol-1-ol is obtained by the reaction of nitropentafluorobenzene with hydrazine hydrate." @default.
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- W2013372014 date "1970-01-01" @default.
- W2013372014 modified "2023-09-30" @default.
- W2013372014 title "Polyfluoroarenes. Part XII. Some azoxy-compounds and benzotriazoles" @default.
- W2013372014 doi "https://doi.org/10.1039/j39700001519" @default.
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