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- W2013632285 abstract "SULPHATION procedures involving the use of 35S-chlorosulphonic acid and 35S-sulphuric acid have been widely applied in the chemical synthesis of 35S-labelled sulphate esters of carbohydrates1, amino-acids2,3 and phenols4,5. A constantly recurring feature of these procedures is that a relatively small proportion only of the 35S-labelled starting material is consumed during the preparation of the required ester, the remainder eventually being removed from the products of reaction as ‘waste’ Ba35SO4. Thus, in a typical preparation of 35S-tyrosine O-sulphate2 using 44 mc. of concentrated H235SO4 as sulphating agent, 38.27 mc. of 35S was eventually recovered as Ba35SO4. In general, Ba35SO4 has only limited use in biological tracer experiments, and in consequence, several methods have been devised for the conversion of this material to a form more suitable for such studies6. The present report describes a method for the conversion of Ba35SO4 to the useful sulphating agent 35S-chlorosulphonic acid." @default.
- W2013632285 created "2016-06-24" @default.
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- W2013632285 date "1962-11-01" @default.
- W2013632285 modified "2023-09-25" @default.
- W2013632285 title "Preparation of 35S-Chlorosulphonic Acid from ‘Waste’, Ba35SO4" @default.
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- W2013632285 doi "https://doi.org/10.1038/196580a0" @default.
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