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• W2013758025 abstract "Abstract [K + (2,2,2‐crypt)] 2 Ge 9 2– containing the deltahedral Zintl anion Ge 9 2– has been isolated from a solution of K 4 Ge 9 in ethylenediamine in the presence of 2,2,2‐crypt, intended as an intermediate in mixed‐cluster synthesis. The subsequent crystallographic characterisation shows the closo ‐Ge 9 2– cluster unit to be tricapped trigonal‐prismatic with a symmetry very close to D 3 h . Each Ge 9 2– unit is surrounded by two 2,2,2‐crypt units, each with a chelated K + cation, viz. [K + (2,2,2‐crypt)]. The structure characterisation of this ordered Ge 9 2– cluster is surprisingly enough the first one reported. A chemical bonding analysis reveals two local minima of D 3 h symmetry, with that of lowest energy being highly similar to that resulting from the crystallographic analysis of low‐temperature data. The cluster interaction scheme is based on highly delocalised bonding." @default.
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• W2013758025 date "2011-07-13" @default.
• W2013758025 modified "2023-10-04" @default.
• W2013758025 title "Structural Investigation of a Fully Ordered <i>closo</i>‐Ge₉^2– Cluster in the Compound [K⁺(2,2,2‐crypt)]₂Ge₉^2–" @default.
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• W2013758025 doi "https://doi.org/10.1002/ejic.201100447" @default.
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