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- W2013865619 abstract "Die Synthese des im Cholinteil deuterierten 3-sn-Phosphatidylcholins 15 und des isomeren 2-Phosphatidylcholins 17 wird beschrieben. Ausgangsprodukte sind die entsprechenden Di-O-acylglycerine 8 bzw. 10, aus denen 15 bzw. 17 über die 1,3,2-Dioxaphospholane in reiner Form aufgebaut werden. Die Bestimmung des Deuterierungsgrades durch kombinierte Auswertung von 1H- NMR-Spektren und FD-Massenspektren wird eingehend diskutiert. Synthesis of 3-sn- and 2-Phosphatidylcholins, Deuterated in the Cholin Part. The synthesis of 3-sn-phosphatidylcholin 15 and of 2-phosphatidylcholin 17 is described. The synthetic pathways start from the respective di-O-acylglycerols 8 and 10 yielding 15 and 17 via the 1,3,2-dioxaphospholanes 14 and 16, respectively. The combination of the data from 1 H NMR spectroscopy and FD mass spectroscopy allows an accurate determination of the degree of deuteration." @default.
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- W2013865619 date "1983-01-01" @default.
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- W2013865619 title "Synthese von im Cholinteil deuterierten 3-sn- und 2-Phosphatidylcholine" @default.
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- W2013865619 doi "https://doi.org/10.1002/jlcr.2580200115" @default.
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