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- W2013894927 abstract "Abstract 2-Cyclohexene-1,2-dicarboxylic acid-anhydride reacts with electron-rich nickel(0) centres to form nickel(0) complexes, whereas the isomeric 4-cyclohexene-1,2-dicarboxylic acid-anhydride reacts with ring opening of the anhydride to yield thermally stable acyl-carboxylato-nickel(II) compounds. The structure of a typical compound with (TMED)Ni 0 as a complex fragment was determined by single crystal X-ray structural analysis, the crystal also containing the product of CO-elimination, the nickelalactone. The cross-coupling reaction of metallacyclic acyl-carboxylato complexes of Ni with RX can be used for the formation of side chains of steroids containing γ-ketocarboxylic acids. These compounds are interesting precursors for the preparation of a analogues of vitamin D3 metabolises." @default.
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- W2013894927 date "1993-03-01" @default.
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- W2013894927 title "Metallacyclische acyl-carboxylate des nickels: Reaktivität der acylgruppe und synthesepotential bei kreuzkopplungsreaktionen mit alkylhalogeniden" @default.
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- W2013894927 doi "https://doi.org/10.1016/0022-328x(93)80282-g" @default.
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