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- W2014043327 abstract "Silica sulfuric acid has been utilized as an efficient heterogeneous recyclable catalyst for Knoevenagel condensation between poorly reactive β-diketones and aldehydes under solvent-free conditions. This protocol also works well with more reactive β-ketoesters. The condensation is efficient, clean, and mild. The scope and generality of the Knoevenagel condensation were investigated. The procedure led only to the Knoevenagel product, and no side product derived from a subsequent Michael addition of β-diketone to alkene was detected at rt. Increasing temperature led to a subsequent Michael addition, and it was applied to the efficient synthesis of 9-aryl-1,8-dioxo-octahydroxanthene derivatives." @default.
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- W2014043327 date "2011-01-25" @default.
- W2014043327 modified "2023-09-24" @default.
- W2014043327 title "Efficient Solvent-Free Knoevenagel Condensation Between β-Diketone and Aldehyde Catalyzed by Silica Sulfuric Acid" @default.
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- W2014043327 doi "https://doi.org/10.1080/00397910903576594" @default.
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