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- W2014050480 abstract "Zinc oxide (ZnO) is a unique material which has been used in many researches. However synthesizing nanosize ZnO remains a challenge. This deal with the preparation of ZnO nanoparticles was synthesized by a self-combustion technique. In the self-combustion technique, nanoparticles was obtained by heating the materials until the mixture combusts at 110°C. ZnO nanoparticles were synthesized from Zn (NO 3 ) 2 .6H 2 O precursor observed in two different solvent. The first set of experiment involved dissolving Zn (NO 3 ) 2 .6H 2 O in nitric acid (HNO 3 ) and adding ZnO, whereas for the second Ethylene Glycol (C 2 H 6 O 2 ) was used as the solvent. The material was stirred at 250 r.p.m continuously for 1 month and 3 days. The mixture was then heated up until it combusted at 110°C. Samples were then annealed at 400°C for 1 hour . The ZnO samples were characterized using X-Ray Diffraction (XRD), Raman Spectroscopy, and Field Emission Scanning Electron Microscope (FESEM). The XRD analysis showed major peak at 20-30 of 2 theta scale with [10, [00, and [10 plane of the wurtzite hexagonal structure for both sets of ZnO samples. Samples were observed at raman shift for 138 and 439 cm -1 and 141 and 443 cm -1 before and after annealing. Synthesized ZnO 1 resulted the morphology of single crystal nanorods with average dimensions of 18 nm wide and 154 nm long. ZnO 2 has obtained the morphology of single crystal nanosphere with average diameter of 30 nm. Keywords: Zinc Oxide, Ethylene Glycol, Self-Combustion Technique" @default.
- W2014050480 created "2016-06-24" @default.
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- W2014050480 date "2014-01-01" @default.
- W2014050480 modified "2023-10-16" @default.
- W2014050480 title "Synthesis and Characterization of Zinc Oxide Nanoparticles via Self-Combustion Technique" @default.
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- W2014050480 doi "https://doi.org/10.4028/www.scientific.net/amm.493.609" @default.
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