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- W2014074938 abstract "Rapid high-performance liquid chromatographic analysis and displacement purification of melittin and its variants were carried out by reversed-phase chromatography. High speed of separation was achieved by the use of columns packed with a micropellicular stationary phase consisting of a thin C18 hydrocarbonaceous layer on the surface of 2-μm fluid-impervious silica microspheres at elevated temperature. In the case of melittin from bee venom or its synthetic variants the plots of the logarithmic retention factor against acetonitrile concentration in the eluent straight lines whereas the van't Hoff plots in the temperature range from 20 to 80°C were non-linear. Purification of melittins by displacement was carried out with benzyldimethylhexadecyl ammonium chloride as the displacer. In a 20-min displacement run at 40°C about 5 mg of highly pure melittin were isolated from 10 mg of synthetic mixture by using a 105 × 4.6 mm column. The results demonstrate that columns packed with micropellicular sorbents not only facilitate rapid high-performance liquid chromatographic analysis but are also suitable for fast peptide purification with high recovery." @default.
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- W2014074938 date "1992-06-01" @default.
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- W2014074938 title "Rapid displacement chromatography of melittin on micropellicular octadecyl-silica" @default.
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- W2014074938 doi "https://doi.org/10.1016/0021-9673(92)85527-z" @default.
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