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- W2014080785 abstract "A method of calibrating retention volumes according to MM in GPC using specimens of any degree of polydispersion, characterized by any mean MM or intrinsic viscosity has been developed. The method is applied to PMMA, but because of the impaired resolution of the chromatographic column in the region of high MM it was impossible to obtain a calibration plot in the form of a linear transformation of a PS calibration true for all values of the MM range. Two calibrations are obtained for the ranges M < 106 and (0·7−3·0) × 106. On the basis of these a single calibration plot was constructed for the whole MM range, which is a non-linear transformation of the PS calibration plot. The relation obtained for solutions of PMM in THF is [η] = 7·3 × 10−5M0.746." @default.
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- W2014080785 date "1987-01-01" @default.
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- W2014080785 title "Calibration of a gel chromatograph for determining the molecular weights of polymethylmethacrylate and little studied polymers" @default.
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- W2014080785 doi "https://doi.org/10.1016/0032-3950(87)90103-1" @default.
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