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- W2014089724 abstract "We report on the fluorous-assisted synthesis of oligosaccharides using a phenyl ether linker. The phenyl ether linker is stable under both acidic and basic conditions but can be cleaved under mildly acidic conditions after reduction to a vinyl ether. The utility of the method was demonstrated by the synthesis of a trisaccharide. A protected trisaccharide with a light-fluorous tag was directly prepared by one-pot glycosylation using three building blocks that contained a building block with a light-fluorous tag though a phenyl ether. A Birch reduction of the trisaccharide provided a fully deprotected trisaccharide with the fluorous tag attached through a vinyl ether, which was easily purified by solid-phase extraction. The tag was cleaved from the sugar portion by treatment with 3% TFA in MeOH." @default.
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- W2014089724 creator A5070398233 @default.
- W2014089724 date "2004-06-01" @default.
- W2014089724 modified "2023-10-15" @default.
- W2014089724 title "Carbohydrate-to-carbohydrate interaction in basic cell biology: a brief overview" @default.
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- W2014089724 doi "https://doi.org/10.1016/j.abb.2004.02.032" @default.
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