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- W2014098679 abstract "The precursors to fluorozirconate glass, which were tested, are volatile β-diketonate complexes. They have all been prepared and characterized (elemental analysis, infrared (IR), nuclear magnetic resonance (NMR), X-ray diffraction, and thermogravimetric analysis (TGA)). La(DPM)3, Al(DPM)3 and Na(HPM), [DPM(H): 2,2,6,6-tetramethyl-3,5-heptanedione, HPM(H): 1,1,1,2,2,3,3-heptafluoro-7,7-dimethyl-4,6-octanedione] are thermally stable, whereas Zr(DPM)3Cl and Ba(HPM)2 are not; Zr(DPM)4 is not volatile enough at the chemical vapour deposition (CVD) reaction temperature. Deposition of AlF3, LaF3 and NaF fluorides has been performed by vapour phase reaction of their precursors with HF or NF3. Starting from an equimolar mixture of the three complexes, a non-homogeneous amorphous material which combines these three fluorides has been deposited. Scanning electron microscope analysis showed carbon impurities." @default.
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- W2014098679 date "1995-05-01" @default.
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- W2014098679 title "Preparation in vapour state of fluoride glass components by a chemical vapour deposition process" @default.
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- W2014098679 doi "https://doi.org/10.1016/0022-3093(95)00006-2" @default.
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