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• W2014099102 abstract "The novel hexanuclear oxoclusters of the general formula R[Mo6O12(OCH3)4(acac)3] (1–7), where R=CH3NH3 (1), C5H5NH (2), (CH3)2CHNH3 (3), (CH3)3CNH3 (4), C5H11NH (5), (C2H5)3NH (6), and C6H5NC11H13O2 (7) have been obtained by the reactions of the binuclear oxomolybdenum(V) complex [Mo2O3(acac)4] (acac=acetylacetonate ion) with a variety of alkyl or aryl amines or corresponding alkyl or aryl ammonium chlorides in methanol. The formation of 3,5-diacyl-2,6-dimethyl-1-pheny-l-pyridinium cation in 7 is explained by the cyclization via Hantzsch condensation of acetylacetone, formaldehyde and aniline. The molecular structures of complexes 5, 6 and 7 have been determined by a single-crystal X-ray diffraction study. In all salts the anion is of hexanuclear nature in which molybdenum atoms are bridged by oxo-oxygen and methoxo-oxygen atoms. Six Mo-octahedra are fused through edges, thus allowing the formation of localized metalmetal bonds between three pairs of molybdenum atoms." @default.
• W2014099102 created "2016-06-24" @default.
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• W2014099102 date "2000-06-01" @default.
• W2014099102 modified "2023-09-24" @default.
• W2014099102 title "Hexanuclear complexes of molybdenum(V) containing [Mo6O12(OCH3)4(acac)3]− anion" @default.
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• W2014099102 doi "https://doi.org/10.1016/s0277-5387(00)00405-8" @default.
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