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• W2014118859 abstract "The reaction of 2 moles of tris(2-aminoethyl)amine and 3 moles of 4-methyl-2,6 diformyl phenol in acetonitrile solution affords a light yellow crystalline solid having composition of H3L, which on reacting with manganese(II) acetate tetrahydrate in alkaline methanol produced the binuclear complex [MnII2L]+. This has been isolated as a perchlorate salt. The X-ray structure of [MnII2L]ClO4·H2O is reported. The lattice consists of two crystallographically independent but metrically very similar binuclear units. Manganese(II) ions are tris μ2-phenolato bridged and the distorted octahedral metal coordination spheres are of type MnN3O3. The frozen (77 K) EPR spectrum of the complex shows group of 11 hyperfine lines with coupling constants of 43.7 G showing that the unpaired electrons interact with both 55Mn centres. The complex displays two successive oxidation couples with E12 values 0.54 and 1.07 V vs saturated calomel electrode." @default.
• W2014118859 created "2016-06-24" @default.
• W2014118859 creator A5032668734 @default.
• W2014118859 creator A5048882099 @default.
• W2014118859 date "1994-01-01" @default.
• W2014118859 modified "2023-10-14" @default.
• W2014118859 title "Synthesis, structure, EPR and electrochemical studies of a μ2-phenoxo bridged manganese(II) dimer afforded by a binucleating macrocylic ligand" @default.
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• W2014118859 doi "https://doi.org/10.1016/s0277-5387(00)84746-4" @default.
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