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• W2014136329 abstract "Abstract With the aim of investigating kraft lignin as a raw material for carbon fibre production, different lignins have been stabilised in air at conditions varied according to a full factorial experimental design. The lignins under examination were purified kraft lignin powders originating from birch, spruce/pine and Eucalyptus globules , as well as lignin fibres originating from birch with 5% poly(ethylene oxide) (PEO) added as a plasticiser. The influence of temperature, time and heating rate on yield and glass-transition temperature (T g ) was investigated. The highest yield was achieved after stabilisation at 280°C during 2 h with a heating rate of 0.2°C min -1 . The T g of all lignin powders was increased when stabilisation occurred under harsher conditions. X-ray photoelectron spectroscopy analysis (XPS) of both the outer surface and the cleaved cross-section of individual lignin/PEO fibres showed a clear gradient in the degree of chemical modification, with the major change occurring on the surface resulting in the appearance of a skin-core structure after stabilisation. The behaviour of the lignin fibres during stabilisation is similar to that of pitch-based fibres, indicating good possibilities for lignin as raw material for carbon fibre production." @default.
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• W2014136329 date "2011-08-06" @default.
• W2014136329 modified "2023-10-16" @default.
• W2014136329 title "Oxidative stabilisation of kraft lignin for carbon fibre production" @default.
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• W2014136329 doi "https://doi.org/10.1515/hf.2011.133" @default.
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