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• W2014155433 startingPage "8918" @default.
• W2014155433 abstract "In this work, we reported an approach for the site-selective growth of nanoparticle onto the tip apex of an atomic force microscopy (AFM) probe. The silicon AFM probe was first coated with a self-assembled monolayer (SAM) of octadecyltrichlorosilane (OTS) through a chemical vapor deposition (CVD) method. Subsequently, COOH groups were selectively generated at the tip apex of silicon AFM probes by applying an appropriate bias voltage between the tip and a flat gold electrode. The transformation of methyl to carboxylic groups at the tip apex of the AFM probe was investigated through measuring the capillary force before and after electrochemical oxidation. To prepare the nanoparticle terminated AFM probe, the oxidized AFM probe was then immersed in an aqueous solution containing positive metal ions, for example, Ag+, to bind positive metal ions to the oxidized area (COOH terminated area), followed by chemical reduction with aqueous NaBH4 and further development (if desired) to give a metal nanoparticle-modified AFM probe. The formation of a metal nanoparticle at the tip apex of the AFM probe was confirmed by scanning electron microscopy (SEM) and energy dispersive X-ray analysis (EDXA)." @default.
• W2014155433 created "2016-06-24" @default.
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• W2014155433 date "2008-07-03" @default.
• W2014155433 modified "2023-10-15" @default.
• W2014155433 title "Sequential Electrochemical Oxidation and Site-Selective Growth of Nanoparticles onto AFM Probes" @default.
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• W2014155433 doi "https://doi.org/10.1021/la800380p" @default.
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