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- W2014198404 abstract "A microcrystalline nonstoichiometric nickel hydroxynitrate Ni(OH)1+s(NO3)1−s (0.288 ⩽ s ⩽ 0.452) is studied by Fourier X-ray line profile analysis. Corrections for instrumental broadening are performed by LWL deconvolution method. The application of the Houska and Warren's method (J. Appl. Phys.25, 1503 (1954)), modified by Maire and Méring (Proc. 4th Conference on Carbon, p. 345, Pergamon Press, New York, 1960) indicates that the line broadening of 00l reflections is not only due to a small particle size effect, but also to crystal defects involving variable interlayer spacings. Seven samples with different s values are investigated. The results indicate that the crystallites of all specimens are composed of a similar number of layers. The mean squares of the variation of the interlayer spacings range from 0.0148 to 0.0003. The square roots are decreasing linearly with the s parameter. It is believed that the observed distortions arise from an irregular distribution of nitrate ions from one layer to another. As s increases, a progressive regularization of the number of nitrate ions involved in each layer is assumed. Existence proof of a well-crystallized nickel hydroxynitrate Ni2(OH)3(NO3) results from this study." @default.
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- W2014198404 date "1975-04-01" @default.
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- W2014198404 title "Analyse des profils de raies de diffraction des rayons X d'un hydroxynitrate de nickel non stoechiométrique" @default.
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- W2014198404 doi "https://doi.org/10.1016/0022-4596(75)90146-2" @default.
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