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- W2014277725 abstract "Abstract The albumen glands of the snail Megalobulimus paranaguensis were previously found to contain a branched β- d -galactopyrananan consisting mainly of nonreducing end-groups and 3,6-di- O -substituted residues with smaller proportions of 3- O - and 6- O -substituted units. 13 C-n.m.r. spectroscopy has now shown that 2-aminoethylphosphonic acid ( 1 ) is an additional component and its presence was confirmed by cellulose-plate chromatography. Furthermore, the 2-aminoethylphosphonic acid-substituted oligosaccharides, formed on partial hydrolysis of the polysaccharide, were isolated, examined by fast-atom-bombardment mass spectrometry, and found to have molecular weights consistent with monophosphonic esters of 1 . The 13 C-n.m.r. spectrum of this mixture indicated substitution of d -galactopyranosyl units at O-6 with esters of 1 , and this was confirmed by spectral examination of a monosubstituted d -galactose isolated after strong acid hydrolysis of the polymer. The snail d -galactan contained one ester of 1 for every 34 residues, it was free of other components such as protein, lipid, and nucleic acid, and is the first polysaccharide of this type that has been identified." @default.
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- W2014277725 date "1985-11-01" @default.
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- W2014277725 title "Occurrence of β-d-galactopyranosyl units esterified at O-6 with 2-aminoethylphosphonic acid in the d-galactan of albumen glands of the snail Megalobulimus paranaguensis" @default.
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- W2014277725 doi "https://doi.org/10.1016/s0008-6215(00)90706-7" @default.
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