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• W2014344317 abstract "A method is described for the removal of “sinc wiggles” from spectra obtained by Fourier transforming truncated time-domain signals. The procedure is especially useful when the signal is severely truncated, as in such a case, the use of a conventional apodization function would seriously degrade the resolution. The method is used to remove “sinc wiggles” from cross sections of a two-dimensional carbon-13 proton J spectrum. It is shown that such a spectrum recorded with only five t 1 increments has sufficient resolution to determine the multiplicities of the carbon lines. However, since the t 1 sampling is very restricted, the cross sections are confused by “sinc wiggles” but the multiplicities can be determined once the procedure described has been used to remove these truncation artifacts. By keeping the maximum value of t 1 to the minimum necessary to achieve the desired resolution the sensitivity of the spectrum is maximized. This approach to determining multiplicities is compared with the existing methods and is shown to have several practical advantages." @default.
• W2014344317 created "2016-06-24" @default.
• W2014344317 creator A5000488507 @default.
• W2014344317 date "1984-02-01" @default.
• W2014344317 modified "2023-10-18" @default.
• W2014344317 title "Elimination of truncation artifacts from NMR spectra. Application to carbon-13 multiplicity determination by two-dimensional spectroscopy" @default.
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• W2014344317 doi "https://doi.org/10.1016/0022-2364(84)90310-x" @default.
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