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- W2014382610 abstract "The silylation of thiamphenicol has been investigated. Treatment of thiamphenicol with hexamethyldisilazane or N-trimethylsilylimidazole, either alone or in the presence of trimethylchlorosilane, in acetonitrile or pyridine yields the bis(trimethylsily) (TMS) ether derivative. These procedures, however, cause to some extent the formation of 1-(p-methylsulphonylphenyl)-2-monochloroacetamido-1,3-propanediol. Silylation with N,O-bis(trimethylsilyl)acetamide gives, depending on the solvent used, the mono-, bis- and tris-TMS derivatives." @default.
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- W2014382610 date "1977-04-01" @default.
- W2014382610 modified "2023-09-24" @default.
- W2014382610 title "Preparation of trimethylsilyl derivatives of thiamphenicol" @default.
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- W2014382610 doi "https://doi.org/10.1016/s0021-9673(00)88535-0" @default.
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