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• W2014391353 endingPage "2639" @default.
• W2014391353 startingPage "2632" @default.
• W2014391353 abstract "We synthesized a linear alkane, K35DA, with a main-chain carbon number n = 33 and three functional groups, a carbonyl group in the middle and carboxyl groups at both ends, and studied influences of the functional groups as well as chain length on morphologies of samples prepared by solution-grown and bulk crystallization methods (SG-K35DA and BK-K35DA) from differential scanning calorimetry (DSC), X-ray diffraction, and IR absorption measurements. Data analyses reveal that at room temperature an orthorhombic crystal of type P212121, together with a considerable amount of amorphous fraction, is predominantly realized in BK-K35DA due to the van der Waals force between neighboring long methylene sequences, whereas a monoclinic type of crystal belonging to the same space group (P21/c) as reported for linear dicarboxylic acid crystals with odd carbon numbers is coexistent for SG-K35DA. The crystalline structures appear to be distorted with increasing temperature, as the dipole−dipole interaction between the carbonyl groups tends to be weakened, and both orthorhombic and monoclinic crystals undergo the solid−solid phase transition to the hexagonal crystalline structure at a temperature about 10 K below their respective Tms, which can be regarded as a new example of the Brill transition." @default.
• W2014391353 created "2016-06-24" @default.
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• W2014391353 date "2009-02-16" @default.
• W2014391353 modified "2023-09-24" @default.
• W2014391353 title "Crystal Structures of <i>n</i>-Alkane with Three Functional Groups in the Middle and at Both Ends" @default.
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• W2014391353 doi "https://doi.org/10.1021/jp808176n" @default.
• W2014391353 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/19219977" @default.
• W2014391353 hasPublicationYear "2009" @default.
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