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• W2014694173 abstract "The refined dependence of the peptide NHCαH vicinal coupling constant on the dihedral angle θ have been derived on the basis of the accumulated experimental data. The mean permissible values (in Hz) are approximated by 3JNHCH = 9·4 cos2 θ - 1·1 cos θ + 0·4 An analogous relationship for the sum of two vicinal NHCαH2 coupling constants in the glycyl residue have been calculated from the above dependence. Measurements on N-methylacetamide in various solvents and in the presence of an alkali salt showed the vicinal constant NHCH to vary by not more than ± 3%. Some of the other proposed 3JNHCH(θ) dependencies give too low values for the cis-oriented NH and CαH bonds. This may be due to the fact that in these correlations the data for compounds with cis-amide bonds have been used for 0° ⩽ θ ⩽ 90° region of the dependence." @default.
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• W2014694173 date "1973-01-01" @default.
• W2014694173 modified "2023-09-24" @default.
• W2014694173 title "Refinement of the angular dependence of the peptide vicinal NHCαH coupling constant" @default.
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• W2014694173 doi "https://doi.org/10.1016/0040-4020(73)80031-6" @default.
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