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- W2014712422 abstract "Soil samples were prepared for multi-element analysis using HNO3 leaching or pseudo-total digestion with HNO3, HCl and HF in a microwave oven, both methods requiring 70 min heating time. Two calibration approaches for the soil characterization were also compared: external calibration, combined with internal standardization, and isotope dilution (ID) after appropriate spiking of the soils with a stable isotope mixture prior to sample preparation. Analyses were performed using inductively coupled plasma sector field mass spectrometry (ICP-SFMS). Accurate total elemental concentrations were only obtained for Cd and P using both sample preparation methods in two certified reference materials, NIST SRM 2709 and CCRMP SO-2, as well as comparable values for a Finnish inter-laboratory soil. The pseudo-total digestion method also provided accurate results for As, Be, Co, Fe, Mn, Ni, Pb, Sb, Ti, V and Zn. For Cu in SO-2 and Cr in both certified reference materials, incomplete recoveries were always obtained. In the case of Cr, this is due to difficulties associated with the complete solubilization of refractory minerals." @default.
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- W2014712422 date "2004-01-01" @default.
- W2014712422 modified "2023-10-10" @default.
- W2014712422 title "Effects of sample preparation and calibration strategy on accuracy and precision in the multi-elemental analysis of soil by sector-field ICP-MS" @default.
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- W2014712422 doi "https://doi.org/10.1039/b315283a" @default.
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