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- W2014787663 abstract "Abstract A simple and efficient method for the synthesis of (α‐hydroxymethyl)phosphinic acids in a pyridine and imidazole series from their corresponding aldehydes and aqueous hypophosphorous acid was developed. The same reaction carried out with an excess of aldehyde in the presence of a mineral acid led mainly to the corresponding bis(α‐hydroxymethyl)phosphinic acids in moderate yields. The coordination properties of these compounds towards Cu II ions were determined. Additionally, it was found that [(hydroxy)(2‐pyridyl)‐ and (hydroxy)(4‐pyridyl)methyl]phosphinic acids were easy to cleave in aqueous sulfuric acid solutions, to form phosphorus acid (H 3 PO 3 ) and the corresponding pyridinemethanols. The kinetics of the cleavage reaction was studied. On the basis of the obtained results, a mechanism of the cleavage was formulated.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)" @default.
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- W2014787663 date "2007-07-01" @default.
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- W2014787663 title "New Heterocyclic Mono- and Bis(α-hydroxymethyl)phosphinic Acids: Synthesis and CuII Binding Abilities" @default.
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- W2014787663 doi "https://doi.org/10.1002/ejoc.200700095" @default.
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