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• W2014900575 abstract "Abstract The solubility and incorporation mechanisms of H and various trivalent and divalent cations in synthetic rutile have been investigated. Experiments performed using different bulk Fe 2 O 3 contents demonstrate that Fe 3+ substitutes onto the main Ti site, charge-balanced by oxygen vacancies. Under more reducing conditions in Fe-poor systems, the concentration of Ti interstitials in rutile is increased, resulting in a decrease in H solubility. Variation in the solubility of different oxides in rutile as a function of ionic radius implies substitution onto the main Ti site, probably charge-balanced by oxygen vacancies. To a lesser degree, substitution of trivalent and divalent cations is locally charge-balanced by H incorporation. Variation in OH-stretching frequencies in infrared spectra as a function of composition implies that octahedral defects and structurally-incorporated H are coupled. However, in all samples, some of the H is also decoupled from substitutional impurities, as is evident from an OH-absorption band at 3279 cm –1 . This band corresponds to the main OH band seen in spectra of many natural rutiles, implying that in most rutiles, H defects are decoupled from substitutional defects." @default.
• W2014900575 created "2016-06-24" @default.
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• W2014900575 date "2005-06-01" @default.
• W2014900575 modified "2023-09-27" @default.
• W2014900575 title "Hydrogen and minor element incorporation in synthetic rutile" @default.
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• W2014900575 doi "https://doi.org/10.1180/0026461056930256" @default.
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