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- W2014997008 abstract "Syntheses in the Ca2Sb2O7 – Ca3Mn2+Sb4O14 system were carried out by solid-state reactions. Both the end-members of this system have a weberite-type structure, although Ca2Sb2O7 exhibits orthorhombic symmetry (2O-polytype), whereas the mineral ingersonite (Ca3Mn2+Sb4O14) exhibits a trigonal symmetry (3T-polytype). X-ray powder diffraction analysis proved run products to consist of both -2O and -3T polytypes. Their unit-cell parameters differ from those of the pure end-members suggesting incorporation of excess Ca in the structure of the trigonal Ca3MnSb4O14 as well as of Mn in the orthorhombic Ca2Sb2O7. The extent of Mn ↔ Ca replacement in both phases was estimated by assuming a linear decrease of the unit-cell volume (normalized to the same formula unit) as a function of the Mn content; moreover, the anisotropic variation of the unit-cell volume indicate a site-preference for the Mn incorporation in the structure of the orthorhombic Ca2Sb2O7." @default.
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- W2014997008 date "2011-01-01" @default.
- W2014997008 modified "2023-09-23" @default.
- W2014997008 title "Ca2Sb2O7 – Ca3Mn2+Sb45+O14 pseudo-binary system: Synthesis and characterization by X-ray powder diffraction" @default.
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- W2014997008 doi "https://doi.org/10.1016/j.solidstatesciences.2010.11.013" @default.
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