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• W2015171045 startingPage "1503" @default.
• W2015171045 abstract "Two novel bolaamphiphile based dicarboxylic ligands L1H2 and L2H2 are synthesized by desymmetrizing aromatic anhydrides. The corresponding Cu(II) complexes [Cu(L1) · EtOH]2 (1), [Cu(L2) · (CH3CN)]2 (2) are synthesized and characterized. The crystal structure obtained for (1) and (2) indicates that they are new class of tetralactone type macrocyclic Cu(II) chelate complexes with paddle wheel Cu2-acetate cage structure. The 1:1, Cu(II) and ligand ratio leads into formation of a novel binuclear Cu(II) tetracarboxylate complexes. The macrocyclic chelate ring size in compounds 1 and 2 was altered from [15] membered to [19] membered by introducing phthalyl and diphenyl head groups as discussed in detail. The single crystal X-ray structure shows the Cu(II)⋯Cu(II) distance 2.613(13) Å for 1 and 2.626(13) Å for 2, the corresponding room temperature EPR spectra recorded for powdered polycrystalline samples indicate the existence of Cu(II)⋯Cu(II) dimeric system." @default.
• W2015171045 created "2016-06-24" @default.
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• W2015171045 date "2008-04-01" @default.
• W2015171045 modified "2023-10-18" @default.
• W2015171045 title "New macrocyclic Cu(II)-bischelates with paddle wheel Cu2-acetate cage" @default.
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• W2015171045 doi "https://doi.org/10.1016/j.ica.2007.08.001" @default.
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