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- W2015202990 abstract "Selected bis-mono, -1,2- and -1,3-disubstituted ferrocenes have been prepared, their 13C NMR spectra have been recorded and simulated in part. From 13C1H couplings and chemical shifts methods for peak assignment have been derived: (a) analysis of the fine structure generated by the coupling with protons in α-position of the substituent, (b) evaluation of the numerical value of 1J(CH), and (c) comparison of the δ-values for mono- and di-substituted molecules. The limits of these aids for assignment are discussed. Es wurden ausgewählte bis-mono-, -1,2- und -1,3-disubstituierte Ferrocene dargestellt, ihre 13C-KMR-Spektren aufgenommen und diese teilweise simuliert. Aus den 13C1H-Kopplungen und chemischen Verschiebungen werden Methoden für die Signalzuordnung abgeleitet: (a) Analyse der Feinstruktur hervorgerufen durch Kopplung mit Protonen in α-Stellung des Substituenten, (b) Ermittlung des Betrags von 1J(CH) und (c) Vergleich der δ-Werte von mono- und disubstituierten Molekülen. Die Grenzen dieser Zuordnungshilfen werden diskutiert." @default.
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- W2015202990 date "1975-09-01" @default.
- W2015202990 modified "2023-10-18" @default.
- W2015202990 title "13C-KMR-spektren bis-substituierter ferrocene zur lösung von zuordnungsproblemen" @default.
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- W2015202990 doi "https://doi.org/10.1016/s0022-328x(00)91945-4" @default.
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