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• W2015226708 abstract "Abstract Real-time ATR-FTIR studies on radiation curing of acrylate formulations by a monochromatic 172 nm (Xe 2 *) excimer lamp and a polychromatic medium pressure mercury arc lamp revealed that under oxygen-free curing conditions photopolymerization reactions take place at high reaction rates even in the absence of a photoinitiator. Due to quantum chemical calculations, the excitation of acrylate molecules by high energy photons (having wavelengths λ C photopolymerization reactions. 2D correlation analysis of the ATR-FTIR data makes the irradiation time-dependent correlation between acrylic C C conversion and wavenumber shifts of C O and C O C bonds evident. On a pilot-scale VUV/UV lamp set-up, through cure of acrylate-based nanocomposites of about 50 μm thickness has been performed in the absence of any photoinitiator. Post-curing VUV irradiation of cured acrylate coatings under nitrogen atmosphere resulted in an excitation of C O groups rather than photodegradation. Radical formation via absorption of high energy photons (having wavelengths λ O bonds is assumed yielding a higher network density within thin surface layers via radical recombination reactions. 2D correlation analysis supports the formation of polar C OH groups generated after H abstraction by C O biradicals. Consequently, additional crosslinking reactions within surface-near layers take place via C C bonds between neighboring polymer chains rather than via C O C bonds. Thus, VUV matted acrylate coatings show enhanced surface hardness, improved chemical resistance, and hydrophilic properties." @default.
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• W2015226708 date "2014-06-01" @default.
• W2015226708 modified "2023-09-25" @default.
• W2015226708 title "Photoinitiator-free UV curing and matting of acrylate-based nanocomposite coatings: Part 3" @default.
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• W2015226708 doi "https://doi.org/10.1016/j.porgcoat.2014.03.013" @default.
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