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- W2015233564 abstract "Concurrent sonolysis of iron pentacarbonyl and poly(ethylene glycol)-400 (PEG-400) in hexadecane solvent proceeds via zero-order kinetics and results in Fe nanoparticles encapsulated in PEG-400 (Fe−PEG). The transmission electron microscopy images show Fe−PEG consisting of <3 nm Fe particles that are evenly dispersed in the PEG matrix. Mössbauer and X-ray absorption fine structure/X-ray absorption near-edge structure data reveal an ordered PEG assembly that helps protect the zerovalent Fe core. The Fe nanoparticles in Fe−PEG are superparamagnetic with a magnetization value of 45 emu/g-Fe at 10 KOe. The rheology of the synthesized material shows an unusual increase in viscosity with temperature that is likely due to lower critical saturation temperature phase segregation over 40 °C. The low-temperature mobility of the PEG-400 moiety in Fe−PEG would allow facile ligation of the Fe0 core with biologically and chemically active groups." @default.
- W2015233564 created "2016-06-24" @default.
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- W2015233564 date "2004-07-07" @default.
- W2015233564 modified "2023-10-06" @default.
- W2015233564 title "Synthesis of Zerovalent Nanophase Metal Particles Stabilized with Poly(ethylene glycol)" @default.
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- W2015233564 doi "https://doi.org/10.1021/la0497402" @default.
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