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- W2015252593 abstract "Abstract The determination of trace metals, e.g. Bi, Co, Cu, Fe, Ni, Pb, U, V, Zn, in high-purity aluminium by total reflection X-ray fluorescence (TXRF) following their separation on HMDC-loaded cellulose is described. For preconcentration, trace metals are adsorbed as their hexamethylenedithiocarbamates (HMDC) from acidic aluminium solutions on a reversed-phase cellulose (e.g. acetylated cellulose). The distribution coefficients Kd of the above elements between collector and solution are of the order 104 ml g . Separation factors of ⩾ 105 can be attained using a column or a batch procedure. After preconcentration the trace elements are determined by TXRF (Mo-tube, Ga as an internal standard) and by flame atomic absorption spectrometry (injection technique). Accordingly, the detection limits of the combined TXRF procedure are in the range of 5–20 ng g depending on the chemical blanks (e.g. Fe, Zn) and the relative standard deviations (n = 5) are in the range of 2.3% (Pb) to 14% (Ni). The accuracy of the analytical procedure is confirmed by TXRF determinations in high-purity reference materials." @default.
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- W2015252593 title "Determination of trace elements in high-purity aluminium by total reflection X-ray fluorescence after their separation on cellulose loaded with hexamethylenedithiocarbamates" @default.
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- W2015252593 doi "https://doi.org/10.1016/0584-8547(89)80060-6" @default.
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