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- W2015381844 abstract "Abstract Thermogravimetric analyses (TGA) of YBa 2 Cu 3 O 7− x powders in a 5% H 2 +Ar atmosphere were carried out in order to determi their oxygen contents. Two slope changes in the TGA curve are observed corresponding to the orthorhombic I↔orthorhombic II and orthorhombic II↔tetragonal transformations. The accuracy of this method in the determination of the oxygen stoichiometry was estimated by comparison with the TGA of pure CuO, and was found to be 0.3%. These results support the possibility of using alternatively the simple XRD route with an error in the oxygen determination less than 1%." @default.
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- W2015381844 date "1989-07-01" @default.
- W2015381844 modified "2023-10-03" @default.
- W2015381844 title "Oxygen content determination in the YBa2O7−x compound" @default.
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- W2015381844 doi "https://doi.org/10.1016/0167-577x(89)90112-2" @default.
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