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- W2015395162 abstract "Doubly enriched (13C, 15N) 1-phenyl-3-(α-cyano)benzylidenetriazene, Ph−N*N−NC(C*⋮N)−Ph, did not show 13C−15N splittings in the NMR spectra in solution that would be expected from the presence of a cyclic nitrene in reversible equilibrium, a theory proposed in 1964 by Smith, Krbechek, and Resemann to explain its chemical behavior. Molecular orbital calculations at the 6-31G* level on the core structures (Ph replaced by H) also indicated substantially greater stability for the open-chain compound. Flash photolysis (337 nm) of 1,4-diphenyl-5-azido-1,2,3-triazole in solution led to the open-chain triazene within about 20 ns but with no observable transient absorbing species." @default.
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- W2015395162 date "1998-07-11" @default.
- W2015395162 modified "2023-09-23" @default.
- W2015395162 title "Characterization of Smith's Nitrene and 1-Phenyl-3-(α-cyano)benzylidenetriazene with Theoretical, NMR, and Flash Photolytic Methods" @default.
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- W2015395162 doi "https://doi.org/10.1021/jp981718s" @default.
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