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• W2015603913 abstract "Palladium rich intermetallic compounds of aluminium, gallium and indium have been studied before and after hydrogenation by powder X-ray diffraction and during hydrogenation by in situ thermal analysis (DSC) at hydrogen gas pressures up to 39 MPa and temperatures up to 700 K. Very weak DSC signals and small unit cell increases of below 1% for AlPd 2 , AlPd 3 , GaPd 2 , Ga 5 Pd 13 , In 3 Pd 5 , and InPd 2 suggest negligible hydrogen uptake. In contrast, for both tetragonal modifications of InPd 3 (ZrAl 3 and TiAl 3 type), heating to 523 K at 2 MPa hydrogen pressure leads to a rearrangement of the intermetallic structure to a cubic AuCu 3 type with an increase in unit cell volume per formula unit by 3.6–3.9%. Gravimetric analysis suggests a composition InPd 3 H ≈0.8 for the hydrogenation product. Very similar behaviour is found for the deuteration of InPd 3 . In situ differential scanning calorimetry of the hydrogenation of tetragonal InPd 3 (ZrAl 3 type) at 1.3 MPa hydrogen pressure." @default.
• W2015603913 created "2016-06-24" @default.
• W2015603913 creator A5016256137 @default.
• W2015603913 date "2010-02-01" @default.
• W2015603913 modified "2023-10-17" @default.
• W2015603913 title "Hydrogenation of palladium rich compounds of aluminium, gallium and indium" @default.
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• W2015603913 doi "https://doi.org/10.1016/j.jssc.2009.11.029" @default.
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