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- W2015643444 abstract "Regioregular head-tail poly(3-hexylthiophenes) (HT-P3HT) with a controlled high molecular weight and a small polydispersity have been synthesized via an improved Kumada catalyst-transfer polycondensation (KCTP) by using the new-prepared hexylmagnesium bromide as the Grignard reagent. As the amount of nickel catalyst dichloro[1,3-diphenylphosphinopropane] nickel (Ni(dppp)Cl2) was 0.5% mol of the amount of monomer 2,5-dibromo-3-hexylthiophene (DBHT) we can obtain a HT-P3HT with a high molecular weight Mn (38 449) and a small polydspersity (1.18). By using of LiCl as a co-catalyst, the regioregularity of the P3HT with high molecular weight (40 270) is maintained and the PDI (1.03) is smaller than that of the P3HT polymerized in the absence of LiCl but the conversion ratio of the monomer is promoted. The HT-P3HT with high molecular weight and small polydispersity will be an attractive candidate applied in solar cells." @default.
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- W2015643444 date "2012-12-01" @default.
- W2015643444 modified "2023-09-27" @default.
- W2015643444 title "Synthesis of Poly(3-Hexylthiophene) with High Molecular Weight and Small Polydispersity" @default.
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- W2015643444 doi "https://doi.org/10.4028/www.scientific.net/amr.616-618.1693" @default.
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