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• W2015665227 abstract "New o-xylylene-linked bis(benzimidazolium) salts were synthesized in six-steps from C2-symmetric chiral 1,4-diol, 1,2-bis(1-hydroxypropyl)benzene, as a starting material. The silver complex of bis(benzimidazol-2-ylidene) was obtained on treatment of bis(benzimidazolium) salt with silver oxide. The reaction of the silver bis-NHC with [PdCl2(PhCN)2] afforded the bis-NHC complex of palladium. The X-ray diffraction studies on Pd complexes revealed that these complexes have distorted square planar geometry around the Pd center coordinating the NHC ligand in mutually cis-position. The arene ring of o-xylylene unit hanged over the Pd center and thus these complexes showed C1-symmetric structures. The variable temperature NMR spectroscopy revealed that these Pd complexes showed fluxional behavior between C1- and C2-symmetric structures in solution state." @default.
• W2015665227 created "2016-06-24" @default.
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• W2015665227 date "2011-06-01" @default.
• W2015665227 modified "2023-10-16" @default.
• W2015665227 title "Synthesis of bis(N-heterocyclic carbene) palladium complexes derived from (S,S)-1,2-bis(1-hydroxypropyl)benzene" @default.
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• W2015665227 doi "https://doi.org/10.1016/j.jorganchem.2011.03.001" @default.
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