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• W2015691889 abstract "The competitive formation of the zeolites ferrierite and dodecasil-3C has been studied under a variety of synthetic conditions involving HF/pyridine as a solvent together with other amines. Single crystal X-ray diffraction measurements on the siliceous zeolite ferrierite product (Si18O36·1.9C5H5N·0.1C3H9N, space group Pmnn, a = 18.8273(6) A, b = 14.095(1) A, c = 7.4318(7) A, V = 1972.2(3) A3, Z = 2, R = 3.1%) reveal that it contains pyridine in both channels. Small amounts of propylamine are found in the main channel. The dodecasil-3C, by contrast, contains pyridine in the larger cavities and propylamine in the smaller ones (Si17O34·0.8C5H5N·0.25C3H9N, space group I42d, a = 13.639(2) A, c = 19.512(4) A, V = 3629.67(6) A3, Z = 4, R = 6.8%). Both the synthetic observations and our computer simulations indicate that the dodecasil-3C is thermodynamically more stable than the ferrierite product, which forms under kinetic control at lower temperatures or shorter reaction times. An additional phase, identified a..." @default.
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• W2015691889 date "1996-01-01" @default.
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• W2015691889 title "Structure-Directing Effects in Zeolite Synthesis: A Single-Crystal X-ray Diffraction, ²⁹Si MAS NMR, and Computational Study of the Competitive Formation of Siliceous Ferrierite and Dodecasil-3C (ZSM-39)" @default.
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• W2015691889 doi "https://doi.org/10.1021/ja952418g" @default.
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