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- W2015704787 abstract "Precipitates of ‘hydrous’ cobalt oxide have been prepared by reacting cobaltous chloride and sodium hydroxide under controlled conditions of pH, concentration and flow rate. The samples were washed and dried at room temperature and small portions heated at controlled temperatures up to 900°. X-Ray analysis of the unheated precipitate indicated that it was possibly a basic chloride of indefinite composition, rather than Co(OH)2. Heat treatment over the range 400°—900° gave Co3O4, the crystallinity increasing with temperature; some CoO was also detected in the 900° sample. The unheated material had an appreciable specific surface area (> 110 m.2/g.), but this decreased rapidly with the temperature of heat treatment and became very low (< 1 m.2/g.) at 900°. The shape of the nitrogen adsorption isotherm changed after heat treatment and the preliminary results suggest that the oxide surface became either more uniform or covered with a chemisorbed layer of oxygen." @default.
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- W2015704787 date "2007-05-04" @default.
- W2015704787 modified "2023-09-23" @default.
- W2015704787 title "The surface properties of precipitated and calcined cobalt oxide" @default.
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- W2015704787 doi "https://doi.org/10.1002/jctb.5010150802" @default.
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