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• W2015886136 abstract "N-Monosubstituted 1,3-diamines were selectively functionalized at the secondary N-atom via 2-Ph-substituted hexahydropyrimidine intermediates. Reaction of the diamines with benzaldehyde, followed by treatment with an electrophile and hydrolysis, provided the desired products with excellent selectivity and in high yields. N4,N9-bis[3-phenylprop-2-enoyl]spermine (4a), which was further converted to N1,N1 2-bis[3-phenylprop-2-enoyl]spermine (15) by a transamidation reaction, was prepared by this way in 82% yield from spermine (1). Compound 4a was alternatively synthesized in 83% yield, equally from 1, by a sequence involving intermediary protection of the terminal amino groups." @default.
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• W2015886136 date "1997-05-12" @default.
• W2015886136 modified "2023-09-26" @default.
• W2015886136 title "Selective Synthesis of Polyamine Derivatives: Efficient derivatization of the secondary amino group ofN-monosubstituted 1,3-diamines" @default.
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• W2015886136 doi "https://doi.org/10.1002/hlca.19970800328" @default.
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